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Articles 8221 - 8250 of 8897

Full-Text Articles in Physical Sciences and Mathematics

The Study On Fabricating Thin Electrodes For Polymer Electrolyte Membrane Fuel Cells(Pemfc), Yong-Sheng Yang, Jing-Hua Liu, Chang-Peng Liu, Gong-Quan Sun, Chang-Zhi Li, Tian-Hong Lu Feb 2000

The Study On Fabricating Thin Electrodes For Polymer Electrolyte Membrane Fuel Cells(Pemfc), Yong-Sheng Yang, Jing-Hua Liu, Chang-Peng Liu, Gong-Quan Sun, Chang-Zhi Li, Tian-Hong Lu

Journal of Electrochemistry

To lower platinum loading in electrodes for polymer electrolyte membrane fuel cell,a new thin electrode fabrication technique(TEFT) was developed in this work.A series of low Pt loading electrodes with smooth and uniformed surface were fabricated by the TEFT.As a result,the maximum power density of the cell with platinum loading of 1 mg/cm 2 and Nafion 117 membrane as electrolyte was up to 0.3 W.cm -2 .Moreover,the effects of PTFE and Nafion content in cathodes on the performance of PEMFC with low Pt loading electrodes(1 mg Pt/cm 2)were examined systematically.

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Studies Of The Preparation Of Electrodes From Lead Carbonate For Lead-Acid Battery Ⅱ.The Preparation Of Paste Electrodes, Zhong-Xu Dai, Di-Hua Wang, Hao-Hao Ke, Jin-Yun Zou, Yun-Hong Zhou Feb 2000

Studies Of The Preparation Of Electrodes From Lead Carbonate For Lead-Acid Battery Ⅱ.The Preparation Of Paste Electrodes, Zhong-Xu Dai, Di-Hua Wang, Hao-Hao Ke, Jin-Yun Zou, Yun-Hong Zhou

Journal of Electrochemistry

The positive and negative pastes were prepared by mixing PbCO 3 and H 2SO 4 solution as well as relative additives, respectively. The effects of the various formation methods and the charge/discharge conditions on discharge capacity and active material utilization of both electrodes were examined. The results indicate that the performance of the positive electrode formed at 2.0 mA/cm 2 is better than that formed at higher current density under the same charge/discharge condition, the PAM utilization reaches 74.4 % under discharging at 2.0 mA/cm 2; and the property of the negative electrode formed by unsymmetrical square wave is superior …

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Effect Of Different Species Of Cobalt Additive On Performance Of Nickel Hydroxide Electrode, Xian-Xia Yuan, Yin-Dong Wang, Feng Zhan Feb 2000

Effect Of Different Species Of Cobalt Additive On Performance Of Nickel Hydroxide Electrode, Xian-Xia Yuan, Yin-Dong Wang, Feng Zhan

Journal of Electrochemistry

Performances of nickel electrodes when adding or without adding Cobalt in different forms were studied, the results were interpreted by cyclic voltammetry(CV)and electrochemical impedance spectroscope(EIS). It was demonstrated that the additions of Co,CoO,CoO+Co by mechanically mixing with Ni(OH) 2 all can improve the performance of nickel electrode to some extent,and when Co is added in the form of CoO the best performance can be obtained. This can be mainly attributed to the fact that three kinds of Co additives all improved the structure of nickel hydroxide and the ability of H + in electrolyte transporting through the material,hence the reversibility …

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Fabrication And Examination Of Reduced Temperatrue Solid Oxide Fuel Cell Using A Supported Thin Ysz Electrolyte Substrate, Yi-Huang Zhang, Yong-Lei Dong, Yi Jiang, Zhi-Gui Lu, Jing-Wang Yan Feb 2000

Fabrication And Examination Of Reduced Temperatrue Solid Oxide Fuel Cell Using A Supported Thin Ysz Electrolyte Substrate, Yi-Huang Zhang, Yong-Lei Dong, Yi Jiang, Zhi-Gui Lu, Jing-Wang Yan

Journal of Electrochemistry

By using a cost_effective wet process,dense yttria stabilized zirconia (YSZ) films on Ni_YSZ anode substrates have been prepared successfully.The YSZ film was characterized to be around 10 μm in thickness,sufficiently dense,uniform and crack free.A single solid oxide fuel cell fabricated from the supported YSZ film electrolyte on the anode substrate and a LSM cathode prepared on the YSZ film was tested.The power density reached to 0.1 W/cm 2 at 800 ℃,showing a reasonable performance.Further analysis on both electrodes shows that the anodic overpotential was much larger than IR drop (including YSZ resistance and contact resistance) and than the cathodic overpotential.The …

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Sprayed And Thermally Evaporated Carbon Films As Anodes For Lithium Ion Batteries, Shu-Gao Zhang, M.Schleich Donald Feb 2000

Sprayed And Thermally Evaporated Carbon Films As Anodes For Lithium Ion Batteries, Shu-Gao Zhang, M.Schleich Donald

Journal of Electrochemistry

Carbon films were made using spray_thermal evaporation from a kind of pyrolytic carbon powder. The films obtained with graphite structure were both potentio_statically and galvanostaically tested. Cycling patterns indicated a reduction peak on the first cycle corresponding to the formation of solid electrolyte interface, and the capacity values and x values were quite acceptable compared to theoretical ones when charging_discharging current density was suitable. Based on the experimental results, the obtained carbon films could be used as anode materials for relatively determining the electrochemical performances of cathode materials.

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Cathodic Indirect Electro-Oxidation——Organic Electro-Synthesis Dimethyl Sulfone, Deng-Ping Gu, Rui-Zhi Wang, Hong-Kun Zhang, Xue-Ying Zhang, Wei Li Feb 2000

Cathodic Indirect Electro-Oxidation——Organic Electro-Synthesis Dimethyl Sulfone, Deng-Ping Gu, Rui-Zhi Wang, Hong-Kun Zhang, Xue-Ying Zhang, Wei Li

Journal of Electrochemistry

A cathodic indirect electro_oxidation system was established for indirect electro_oxidize dimethyl sulfoxide to dimethyl sulfone with electro_reduction generated H 2O 2 catalyzed by the pertungstate/tungstate(WO 5 2- /WO 4 2- )redox mediator. Influences of current density,pH,temperature,and the current efficiencies etc. on the cathodic indirect electro_oxidation of dimethyl sulfone were investigated for determining optimum reaction conditions.The current efficiency reached more than 70%.Mother_liquid could be recycled to use without pollution.

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Studies On Electrochemical Synthesis Of 4,5-Disubstituted-1,2- Benzoquinones And The Reaction Mechanism, Xian-Zhang Bu, Gui-Wu Xiao, Lin Ma, Xing-Chum He, Ling-Quan Gu Feb 2000

Studies On Electrochemical Synthesis Of 4,5-Disubstituted-1,2- Benzoquinones And The Reaction Mechanism, Xian-Zhang Bu, Gui-Wu Xiao, Lin Ma, Xing-Chum He, Ling-Quan Gu

Journal of Electrochemistry

The oxidation peak potentials( E p) of alinine derivates and catechol in 0.1 mol/L KCl+15% alcohol solution were measured by cyclic voltammograms technique. The electrochemical oxidation condition was set according to the E p. Three derivates of 4,5_disubstituted _1,2_benzoquinones were prepared via electrochemical oxidation_Michael addition reaction. The possible mechanism of electrochemical oxidation_Michael addition reaction is presented.

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Electrochemical Characterization Of Ir-Ta-Ti Metal Oxide Coated Titanium Anodes, Ting-Yong Wang, Li-Kun Xu, Guang-Zhang Chen Feb 2000

Electrochemical Characterization Of Ir-Ta-Ti Metal Oxide Coated Titanium Anodes, Ting-Yong Wang, Li-Kun Xu, Guang-Zhang Chen

Journal of Electrochemistry

Ir_Ta_Ti metal oxide coated titanium anodes of variable composition were prepared by thermal decomposition. Their micro morphorogies and electrochemical properties were characterized by scanning electron microscope, open circuit potential, cyclic voltammetry, consumption rate measurements and accelerated life test. The SEM results indicated that all coatings were of a porous and cracked_mud microstructure influenced greatly by the composition of coatings. The electrochemical measurements showed that the Ir_Ta_Ti ternary oxide_coated anodes exhibited excellent electrochemical activity and electrochemical stability in both acidic media and seawater which were affected by the composition and microstructure of the coatings. Owing to good corrosion resistance and low …

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Investigations Of Lithium Ion Battery Electrolyte Solution, Jing-Li Han, Qing-Guo Liu Feb 2000

Investigations Of Lithium Ion Battery Electrolyte Solution, Jing-Li Han, Qing-Guo Liu

Journal of Electrochemistry

Synthesis and electrochemical investigations of ｛LiB[(SO 3)C 6H 3(O)(COO)]OC 6H 5｝in EC/DMC or DMSO/PC mixtures are presented.

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Electro-Oxidation Of Glyoxal To Glyoxalic Acid, Yin-Sheng Chen, Xin-Sheng Zhang, Jun Hu, Ying-Chun Dai Feb 2000

Electro-Oxidation Of Glyoxal To Glyoxalic Acid, Yin-Sheng Chen, Xin-Sheng Zhang, Jun Hu, Ying-Chun Dai

Journal of Electrochemistry

An investigation has been made to obtain the glyoxalic acid by the electrochemical oxidation of glyoxal solution with hydrochloric acid under various experimental conditions.The cell used consists of a lead cathode, a DSA anode and a cation_exchange membrane of model CM001.The current efficiency and yield for glyoxalic acid generation were 80.0% and 91.1% respectively, under optimal operating conditions: velocity of electrolyte flow 1.4 m·s -1 ,current density 450A·m -2 ,temperature 30～40 ℃,initial concentration of glyoxal and hydrochloric acid 9.1%～16.0%, 4%～6%, respectively.

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Bottom-Up Design Of Artificial Neural Network For Single-Lead Electrocardiogram Beat And Rhythm Classification, Srikanth Thiagarajan Jan 2000

Bottom-Up Design Of Artificial Neural Network For Single-Lead Electrocardiogram Beat And Rhythm Classification, Srikanth Thiagarajan

Doctoral Dissertations

Performance improvement in computerized Electrocardiogram (ECG) classification is vital to improve reliability in this life-saving technology. The non-linearly overlapping nature of the ECG classification task prevents the statistical and the syntactic procedures from reaching the maximum performance. A new approach, a neural network-based classification scheme, has been implemented in clinical ECG problems with much success. The focus, however, has been on narrow clinical problem domains and the implementations lacked engineering precision. An optimal utilization of frequency information was missing. This dissertation attempts to improve the accuracy of neural network-based single-lead (lead-II) ECG beat and rhythm classification. A bottom-up approach defined …

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Vhdl Design And Simulation For Embedded Zerotree Wavelet Quantisation, Hung Huynh Jan 2000

Vhdl Design And Simulation For Embedded Zerotree Wavelet Quantisation, Hung Huynh

Theses : Honours

This thesis discusses a highly effective still image compression algorithm – The Embedded Zerotree Wavelets coding technique, as it is called. This technique is simple but achieves a remarkable result. The image is wavelet-transformed, symbolically coded and successive quantised, therefore the compression and transmission/storage saving can be achieved by utilising the structure of zerotree. The algorithm was first proposed by Jerome M. Shapiro in 1993, however to minimise the memory usage and speeding up the EZW processor, a Depth First Search method is used to transverse across the image rather than Breadth First Search method as initially discussed in Shapiro's …

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New Free-Space Multistage Optical Interconnection Network And Its Matrix Theory, Fengguang Luo, Mingcui Cao, Anjun Wan, Jun Xu, Xinjun Zhou, Cong Deng Jan 2000

New Free-Space Multistage Optical Interconnection Network And Its Matrix Theory, Fengguang Luo, Mingcui Cao, Anjun Wan, Jun Xu, Xinjun Zhou, Cong Deng

Electro-Optics and Photonics Faculty Publications

A new free-space multistage optical interconnection network which is called the Comega interconnection network is presented. It has the same topological construction for the cascade stages of the Comega interconnection. The concept of the left Comega and the right Comega interconnection networks are given to describe the whole Comega interconnection network. The matrix theory for the Comega interconnection network is presented. The route controlling of the Comega interconnection network is decided based on the matrix analysis. The node switching states in cascade stages of the 8 by 8 Comega interconnection network for the route selection are given. The data communications …

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Characterization Of Poly-Si Thin Films Deposited By Magnetron Sputtering Onto Ni Prelayers, Elena A. Guliants, Wayne A. Anderson Jan 2000

Characterization Of Poly-Si Thin Films Deposited By Magnetron Sputtering Onto Ni Prelayers, Elena A. Guliants, Wayne A. Anderson

Electrical and Computer Engineering Faculty Publications

A method of producing a polycrystalline silicon thin film on a foreign substrate without subsequent annealing has been developed. Thermally evaporated 5–100 nm thick Nifilms served as prelayers for magnetron sputtered Si thin films. A continuous film was obtained as a result of metal induced growth of polysilicon during low temperature (below 600 °C) deposition. The film uniformity is promising for large area device applications. The influence of the Ni prelayer thickness on the grain size of thus obtained films was investigated. Atomic force microscopy and cross-sectional scanning electron microscopy studies revealed features in the 150–600 nm size range while …

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An Efficient Algorithm To Determine The Periodic Steady-State Solutions Of Nonlinear Systems Using Extended Spectral Analysis, Gülay Tohumoğlu Jan 2000

An Efficient Algorithm To Determine The Periodic Steady-State Solutions Of Nonlinear Systems Using Extended Spectral Analysis, Gülay Tohumoğlu

Turkish Journal of Electrical Engineering and Computer Sciences

A new method for the solution of nonlinear periodic systems was developed. It avoids the time domain calculations of the whole network equations. In the proposed method, by forming the augmented network as linear and nonlinear subnetworks these subnetworks are formulated in complex frequency and time domain respectively. Using spectral analysis the steady-state periodic solution of the whole nonlinear network is reached by an iterative approach. The method can be applied efficiently to weak and strong nonlinear circuits equally well. When we divide the network into a large linear subnetwork and a small nonlinear subnetwork, this method can be applied …

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A Pseudo Spot Price Algorithm Applied To The Pumped-Storage Hydraulic Unit Scheduling Problem, Sali̇h Fadil, Celal Yaşar Jan 2000

A Pseudo Spot Price Algorithm Applied To The Pumped-Storage Hydraulic Unit Scheduling Problem, Sali̇h Fadil, Celal Yaşar

Turkish Journal of Electrical Engineering and Computer Sciences

A lossy electric power system that contains thermal units and a pumped-storage hydraulic unit is considered in this paper. The total cost of thermal units in an operation cycle is minimized under some possible electric and hydraulic constraints of the units. The operation cycle is divided into time intervals where the system loads are assumed to remain constant. The proposed solution technique has two main parts. In the first part, the active thermal generations and active generation or pumping power of the pumped-storage unit in all time intervals are determined by using units' active generation incremental costs and pseudo spot …

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Distance Spectra For Trellis Coded Modulation Schemes On Channels With Intersymbol Interference, Sabi̇re Haciömeroğlu, Melek D. Yücel Jan 2000

Distance Spectra For Trellis Coded Modulation Schemes On Channels With Intersymbol Interference, Sabi̇re Haciömeroğlu, Melek D. Yücel

Turkish Journal of Electrical Engineering and Computer Sciences

The effect of intersymbol interference on distance spectra for trellis coded 8-PSK, 16-QAM and 32-AMPM modulation schemes is evaluated using the methods proposed by Schlegel. Distance spectra of 16-state 8-PSK scheme are computed for different intersymbol interference channels. It is seen that on channels with intersymbol interference the spectral lines are spread into a nearly continuous spectrum and the minimum Euclidean distance between codewords decreases severely. Hence, although the main contribution at large signal to noise ratios comes from the minimum Euclidean distance ( d_{free} ) , higher spectral components also become very important at moderate values of the signal …

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Series Operation Of Direct Current Xenon Chloride Excimer Sources, Ahmed El-Habachi, Wenhui Shi, Mohamed Moselhy, Robert H. Stark, Karl H. Schoenbach Jan 2000

Series Operation Of Direct Current Xenon Chloride Excimer Sources, Ahmed El-Habachi, Wenhui Shi, Mohamed Moselhy, Robert H. Stark, Karl H. Schoenbach

Bioelectrics Publications

Stable, direct current microhollow cathode discharges in mixtures of hydrochloric acid, hydrogen, xenon, and neon have been generated in a pressure range of 200–1150 Torr. The cathode hole diameter was 250 μm. Sustaining voltages range from 180 to 250 V at current levels of up to 5 mA. The discharges are strong sources of xenon chloride excimer emission at a wavelength of 308 nm. Internal efficiencies of approximately 3% have been reached at a pressure of 1050 Torr. The spectral radiant power at this pressure was measured as 5 mW/nm at 308 nm for a 3 mA discharge. By using …

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Information And Average Information Rates Of A Graphical Access Structure On Six Vertices, Mustafa Atici Jan 2000

Information And Average Information Rates Of A Graphical Access Structure On Six Vertices, Mustafa Atici

Turkish Journal of Electrical Engineering and Computer Sciences

In this paper we study the optimal information and average information rates of secret sharing schemes which are all connected graphs on six vertices. There are $102$ connected graphs on six vertices that are not complete multipartite graphs. Of these $102$ graphs, we determined the optimal information rate of $71$ graphs, and the optimal average information rate of $88$ graphs.

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Radiation From An Impedance Loaded Parallel-Plate Waveguide, Fi̇li̇z Bi̇rbi̇r, Ali̇nur Büyükaksoy Jan 2000

Radiation From An Impedance Loaded Parallel-Plate Waveguide, Fi̇li̇z Bi̇rbi̇r, Ali̇nur Büyükaksoy

Turkish Journal of Electrical Engineering and Computer Sciences

A hybrid method consisting of employing the mode matching method in conjunction with the Fourier transform technique is used to analyze the radiation of the dominant TEM-wave from an impedance loaded parallel-plate waveguide. The hybrid method that we adopt here reduces the related boundary value problem to a scalar modified Wiener-Hopf equation of the second kind. The solution involves infinitely many unknown constants satisfying an infinite system of linear algebraic equations susceptible to a numerical treatment. Some computational results illustrating the effects of various parameters on the radiation phenomenon are also presented.

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A Fuzzy Identification Method For Nonlinear Systems, İbrahi̇m Eksi̇n, Osman Kaan Erol Jan 2000

A Fuzzy Identification Method For Nonlinear Systems, İbrahi̇m Eksi̇n, Osman Kaan Erol

Turkish Journal of Electrical Engineering and Computer Sciences

In this paper, two mathematical ways of building a fuzzy model of both linear and nonlinear systems are presented and compared. In order to determine a model for a nonlinear system, the phase plane is divided into sub-regions and a linear model is assigned for each of these regions. This linear model is represented either in state-space or ARX model form. To determine the pre-selected parameters of the linear system model under study, least-square identification method is used. Then these linear models are arranged in a fuzzy manner to characterize the overall system behavior. The results show that this method …

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Control Chart Pattern Recognition Using Artificial Neural Networks, Şeref Sağiroğlu, Erkan Beşdok, Mehmet Erler Jan 2000

Control Chart Pattern Recognition Using Artificial Neural Networks, Şeref Sağiroğlu, Erkan Beşdok, Mehmet Erler

Turkish Journal of Electrical Engineering and Computer Sciences

Precise and fast control chart pattern (CCP) recognition is important for monitoring process environments to achieve appropriate control and to produce high quality products. CCPs can exhibit six types of pattern: normal, cyclic, increasing trend, decreasing trend, upward shift and downward shift. Except for normal patterns, all other patterns indicate that the process being monitored is not functioning correctly and requires adjustment. This paper describes a new type of neural network for speeding up the training process and to compare three training algorithms in terms of speed, performance and parameter complexity for CCP recognition. The networks are multilayered perceptrons trained …

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Knowledge-Based Navigation For Autonomous Road Vehicles, Murat Eki̇nci̇, Franches W.J.Gibbs, Barry T. Thomas Jan 2000

Knowledge-Based Navigation For Autonomous Road Vehicles, Murat Eki̇nci̇, Franches W.J.Gibbs, Barry T. Thomas

Turkish Journal of Electrical Engineering and Computer Sciences

This paper presents a computer vision system for an autonomous road vehicle (ARV) that is capable of negotiating complex road networks including road junctions in real time. The ultimate aim of the system is to enable the vehicle to drive automatically along a given complex road network whose geometric description is known. This computer vision system includes three main techniques which are necessary for an ARV: a) road following, b) road junction detection, c) manoeuvring at the road junction. The road following algorithm presents a method of executing a number of algorithms using different methods concurrently, fusing their outputs together …

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Decentralised H_{\Infty} Load Frequency Controller Design Based On Ssvs, Hasan Çi̇men Jan 2000

Decentralised H_{\Infty} Load Frequency Controller Design Based On Ssvs, Hasan Çi̇men

Turkish Journal of Electrical Engineering and Computer Sciences

The decentralised load-frequency controller design problem concerned is translated into an equivalent problem of decentralised controller design for a multi-area multi-input multi-output (MIMO) control system. It is shown that subject to a condition based on the structured singular values (SSVs), each local area load-frequency controller can be designed independently. The stability condition for the overall system can be stated as to achieve a sufficient interaction margin. It is demonstrated by computer simulation that within this general framework, local H$_{\infty}$ controllers can be designed to achieve satisfactory performances for a sample two-area power system.

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Comparison Of Simulation Algorithms For The Hopfield Neural Network: An Application Of Economic Dispatch, Tankut Yalçinöz, Hali̇s Altun Jan 2000

Comparison Of Simulation Algorithms For The Hopfield Neural Network: An Application Of Economic Dispatch, Tankut Yalçinöz, Hali̇s Altun

Turkish Journal of Electrical Engineering and Computer Sciences

This paper is mainly concerned with an investigation of the suitability of Hopfield neural network structures in solving the power economic dispatch problem. For Hopfield neural network applications to this problem three important questions have been answered: what the size of the power system is; how efficient the computational method; and how to handle constraints. A new mapping process is formulated and a computational method for obtaining the weights and biases is described. A few simulation algorithms used to solve the dynamic equation of the Hopfield neural network are discussed. The results are compared with those of a classical technique, …

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Nonlinear Self-Organization In Photorefractive Materials, Partha P. Banerjee, Nickolai Kukhtarev, John O. Dimmock Jan 2000

Nonlinear Self-Organization In Photorefractive Materials, Partha P. Banerjee, Nickolai Kukhtarev, John O. Dimmock

Electrical and Computer Engineering Faculty Publications

This chapter discusses self-organization and its effects in optics. One of the most exciting and potentially useful areas of current research in optics involves the understanding and exploitation of self-organization in nonlinear optical systems. This self-organization may sometimes lead to the evolution of complex spatial patterns that can be regarded as the nonlinear eigenmodes of the system. Generation of these patterns is characteristically marked by the presence of intensity thresholds. In a nonlinear system with complicated temporal dynamics, it turns out that one cannot retain purity in spatial dimensionality. It is therefore equally important to investigate the dynamics of the …

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Low Damage Processing And Process Characterization, Xianmin Tang Jan 2000

Low Damage Processing And Process Characterization, Xianmin Tang

Dissertations, Theses, and Masters Projects

Two novel plasma sources (one neutral source and one pulsed inductively coupled plasma source) and ashing process characterization were investigated. The primary goal was to characterize these source properties and develop corresponding applications. The study includes process damage assessment with these two sources and another continuous wave (13.56MHz) plasma source. A global average simulation of the pulsed discharges was also included.;The transient plasma density and electron temperature from the double probe analysis were compared with single Langmuir probe results with sheath displacement corrections in pulsed discharges (200Hz--10kHz). The equivalent resistance method can be used effectively to analyze these double probe …

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High Performance Proton Exchange Membrane Fuel Cells, Jingrong Yu, Baolian Yi, Ming Han, Xiaoliang Cheng, Zhigang Shao, Jingxin Zhang Nov 1999

High Performance Proton Exchange Membrane Fuel Cells, Jingrong Yu, Baolian Yi, Ming Han, Xiaoliang Cheng, Zhigang Shao, Jingxin Zhang

Journal of Electrochemistry

Proton_exchange membrane fuel cells(PEMFC) using a perfluorosulfonic acid proton exchange membrane as an electrolyte can simplify water and electrolyte management.In this paper,the effects of thickness of PEM on the performance of PEMFC were studied.The Nafion_112 PEM and low platinum loading E_TEK electrode yielded very high power density,of the order of 0.95 W/cm 2.The energy_conversion efficiency,the degree of platinum utilization and stability for PEMFC using Nafion 112 and E_TEK electrode were also investigated.

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Electro Oxidation Of Phenol On Sno_2/Ti Electrodes Prepared By Thermal Oxidation, Qingsong Zhang, Huihuang Wu Nov 1999

Electro Oxidation Of Phenol On Sno_2/Ti Electrodes Prepared By Thermal Oxidation, Qingsong Zhang, Huihuang Wu

Journal of Electrochemistry

A SnO 2/Ti electrode prepared by thermal oxidation was used as the anode for galvanostatic electrolysis in acidic solution containing phenol, the time_dependances of phenol concentration,chemical oxygen demand in solution(COD)and instantaneous current efficiency were determined during electrolysis.The results show that with the SnO 2/Ti anode instead of Pt,the COD significantly decreases at the same charge passage, and average current efficiency of oxidation increases by three times The mechanism for phenol oxidation at two electrodes was discussed.

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Investigation Of Sodium Hypophosphite Anodic Oxidizing Behavior In The Process Of Acid Electroless Nickel Deposition, Meiyuan Wang, Yafei Kuang, Yan Xu Nov 1999

Investigation Of Sodium Hypophosphite Anodic Oxidizing Behavior In The Process Of Acid Electroless Nickel Deposition, Meiyuan Wang, Yafei Kuang, Yan Xu

Journal of Electrochemistry

The anodic oxidizing behavior of sodium hypophosphite in the process of electroless nickle deposition(pH=5.5) was investigated with the linear potential sweep method and alternating current impedance.The results indicated that,the oxidation of NaH 2PO 2 was a complicated electrochemical process and affected by the concentration of NaH 2PO 2, the temperature of the bath,the sweep rate and the existence of nickel ion. The NaH 2PO 2 electrooxidation reaction was very likely preceded by heterogeneous interface transformation process,which might be the control step of the whole anodic process.

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